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The initial preparation, anticipation and implementation of USP 232 to meet heavy metal compliance for oral, injectable and inhalation pharmaceutical products has passed. The time has come for review of limit calculations, microwave sample preparation and ICP‐MS method parameters to optimize the process. Whether your laboratory is considering adoption of in‐house methods or wants a clearer understanding of the process, this webcast will demystify the methodology and present turn‐key processes created by Milestone and Agilent for this heavy metal requirement. We will also cover laboratory reagent and environmental considerations for successfully preparing and measuring low (ppb) concentrations in complex pharmaceutical matrices. Key Learning Objectives • Review the full process for analyzing various pharmaceutical samples, from initial sample preparation to ICP‐MS or ICP‐OES analysis • See how both rotor‐based and single reaction chamber (SRC) digestion technologies can accommodate the needs of pharmaceutical testing laboratories • Learn how and why SRC technology is uniquely suited for the sample preparation needs of the pharmaceutical industry • Understand the important factors for successful metals analysis of pharmaceutical matrices using ICP‐MS or ICP‐OES